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This text for the two-semester introductory organic chemistry lab offers a series of clear and concise experiments that encourage accurate observation and deductive reasoning. A focus on biochemical and biomedical applications renders the narrative ideal for the mainstream organic chemistry laboratory. Emphasis is also placed on safety and the disposal of hazardous waste.
Pre-lab exercises, marginal notes, clear line drawings, and questions help retain student interest and comprehension from lesson to lesson.
Optional, additional "For Further Investigation" features offer an in-depth exploration of the chemical principles presented. Introduction 2. Laboratory Safety and Waste Disposal Techniques 3.
Crystallization 4. Distillation 6. Steam Distillation 7. Vacuum Distillation and Sublimation 8. Infrared Spectroscopy Nuclear Magnetic Resonance Spectroscopy Ultraviolet Spectroscopy and Mass Spectrometry The SN2 Reaction: 1-Bromobutane Nucleophilic Substitution Reactions of Alkyl Halides Alkenes from Alcohols: Cyclohexene from Cyclohexanol Bromination and Debromination: Purification of Cholesterol Dichlorocarbene Oxidation and Reduction Pulegone from Citronellol: Oxidation with Pyridinium Chlorochromate Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol Catalytic Hydrogenation Epoxidation of Cholesterol Aromatic Substitution and Elimination Nitration of Methyl Benzoate Alkylation of Mesitylene Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical Friedel-Crafts Acylation of Ferrocene: Acetylferrocene Triptycene via Benzyne Reactions of aldehydes and Ketones Aldehydes and Ketones Dibenzalacetone by the Aldol Condensation Grignard Synthesis of Triphenylmethanol and Benzoic Acid Esterification and Hydrolysis Acetylsalicylic Acid Aspirin Malonic Ester Synthesis of a Barbiturate Amines Sulfanilamide from Nitrobenzene Dyes and Dyeing Diels-Alder Reaction Ferrocene, [Bis cyclopentadienyl iron] Tetraphenylcyclopentadienone Nitric Acid Oxidation.
Preparation of Benzil from Benzoin. Synthesis of a Heterocycle: Diphenylquinoxaline Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil Synthesis of 2,2-Dimethyl-1,5-dioxolane.
The Acetonide Derivative of a Vicinal Diol Synthesis of an Alkyne from an Alkene. Bromination and Dehydrobromination: Stilbene and Diphenylacetylene Decarboxylation: Synthesis of cis-Stilbene Photochemistry Chemiluminescence: Syntheses of Cyalume and Luminol Carbohydrates and Sweeteners Biosynthesis of Ethanol Isolation of Lycopene and beta-Carotene Polymers: Synthesis and Recycling Qualitative Organic Analysis Searching the Chemical Literature. Ken Williamson is retired from Mt.
Holyoke College where he taught the organic chemistry laboratory course. He is an established authority on microscale techniques and regularly holds workshops and travels to campuses in the U. Convert currency. Add to Basket. Book Description Brooks Cole, Condition: New. More information about this seller Contact this seller. Book Description Condition: New. Brand New. US Edition Book. We do not ship to Military Addresses.
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View all copies of this ISBN edition:. Synopsis About this title This text for the two-semester introductory organic chemistry lab offers a series of clear and concise experiments that encourage accurate observation and deductive reasoning. Review : 1. Buy New Learn more about this copy. About AbeBooks. Other Popular Editions of the Same Title. Search for all books with this author and title.
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Organic Experiments / Edition 9